I-D-Amino Acids Series ye-Solid Phase Synthesis
Imininingwane Yomkhiqizo
| No | Imikhiqizo | Inombolo ye-CAS. | Inkomba yekhwalithi engukhiye | ||||
| Ubumsulwa | Isomer | Ukungcola Okuthize | *Ubukhulu 1 | Umswakama | |||
| 1 | I-Fmoc-D-Ala-OH.H2O | 79990-15-1 | ≥99.5% | ≤0.1% | ≤0.1% | ≤0.2% | ≤6.5% |
| 2 | I-Fmoc-3-(2-naphthyl)-D-Ala-OH | 138774-94-4 | ≥99.0% | ≤0.2% | ≤0.3% | ≤0.3% | ≤1.0% |
| 3 | I-Ac-3-(2-naphthyl)-D-Ala-OH | 37440-01-0 | ≥99.0% | ≤0.2% | ≤0.3% | ≤0.3% | ≤1.0% |
| 4 | I-Fmoc-3-(3-pyridinyl)-D-Ala-OH | 142994-45-4 | ≥99.0% | ≤0.2% | ≤0.3% | ≤0.3% | ≤1.0% |
| 5 | I-Fmoc-D-Aph(tBuCbm)-OH | 1433975-21-3 | ≥99.0% | ≤0.2% | ≤0.3% | ≤0.3% | ≤1.0% |
| 6 | I-Fmoc-D-Aph(Cbm)-OH | 324017-22-3 | ≥99.0% | ≤0.2% | ≤0.3% | ≤0.3% | ≤1.0% |
| 7 | I-Fmoc-D-Aph(Hor)-OH | NA | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 8 | I-Fmoc-Aph(D-Hor)-OH | NA | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 9 | I-Fmoc-D-Arg(pbf)-OH | 187618-60-6 | ≥99.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤2.0% |
| 10 | I-Fmoc-D-Arg (NO2)-OH | 160347-94-4 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤2.0% |
| 11 | I-Fmoc-D-HomoArg(pbf)-OH | 401915-53-5 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤2.0% |
| 12 | I-Fmoc-D-HomoArg(Et)2-OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤2.0% |
| 13 | I-Fmoc-D-Asn(Trt)-OH | 180570-71-2 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 14 | I-Fmoc-D-Asp(OtBu)-OH | 112883-39-3 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 15 | I-Fmoc-D-Asp-OtBu | 34098-70-7 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 16 | I-Fmoc-D-Asp(OAll)-OH | 177609-12-0 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 17 | Fmoc-D-Cit-OH | 200344-33-8 | ≥99.5% | ≤0.1% | ≤0.1% | ≤0.2% | ≤1.0% |
| 18 | I-Fmoc-D-Cys(Trt)-OH | 167015-11-4 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 19 | I-Fmoc-D-Cys(Acm)-OH | 168300-88-7 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 20 | I-Fmoc-D-Cys(Mmt)-OH | 1198791-73-9 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 21 | I-Fmoc-D-Gln(Trt)-OH | 200623-62-7 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤2.0% |
| 22 | I-Fmoc-D-Glu(OtBu)-OH.H2O | 104091-08-9 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤5.0% |
| 23 | I-Fmoc-D-Glu-OtBu | 109745-15-5 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 24 | I-HD-Glu-OtBu | 25456-76-2 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 25 | Fmoc-D-His(Trt)-OH | 135610-90-1 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 26 | Boc-D-His(Trt)-OH | 393568-74-6 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 27 | I-Fmoc-D-His(Bzl)-OH | 1417638-37-9 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 28 | Fmoc-D-Ile-OH | 143688-83-9 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 29 | Fmoc-D-Allo-Ile-OH | 118904-37-3 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 30 | Fmoc-D-Leu-OH | 114360-54-2 | ≥99.5% | ≤0.1% | ≤0.1% | ≤0.2% | ≤1.0% |
| 31 | I-Fmoc-D-Ls(Boc)-OH | 92122-45-7 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 32 | I-Fmoc-D-Ls(Alloc)-OH | 214750-75-1 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 33 | I-Fmoc-D-Ls(ivDde)-OH | 1272755-33-5 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 34 | I-Fmoc-D-Ls(Mmt)-OH | 198544-94-4 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 35 | I-Fmoc-D-Ls(iPr,Boc)-OH | NA | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 36 | I-Fmoc-D-Lys(nicotinoyl)-OH | 252049-12-0 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 37 | I-Fmoc-D-Met-OH | 112883-40-6 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 38 | I-Fmoc-D-Orn(Boc)-OH | 118476-89-4 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 39 | Fmoc-D-Phe-OH | 86123-10-6 | ≥99.5% | ≤0.1% | ≤0.1% | ≤0.2% | ≤1.0% |
| 40 | I-Fmoc-4-chloro-D-Phe-OH | 142994-19-2 | ≥99.0% | ≤0.2% | ≤0.3% | ≤0.3% | ≤1.0% |
| 41 | I-Fmoc-D-Pro-OH.H2O | 101555-62-8 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤6.0% |
| 42 | I-D-Pyr-OH | 4042-36-8 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 43 | I-Fmoc-D-Ser(tBu)-OH | 128107-47-1 | ≥99.5% | ≤0.1% | ≤0.1% | ≤0.2% | ≤1.0% |
| 44 | I-Fmoc-D-Ser(Trt)-OH | 212688-51-2 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 45 | I-Fmoc-D-Thr(tBu)-OH | 138797-71-4 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 46 | I-Fmoc-D-Trp(Boc)-OH | 163619-04-3 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤2.0% |
| 47 | I-Fmoc-2-methyl-D-Trp-OH | 196808-79-4 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤2.0% |
| 48 | I-Fmoc-D-Tyr(tBu)-OH | 118488-18-9 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 49 | I-Fmoc-D-Tyr(Et)-OH | 162502-65-0 | ≥99.5% | ≤0.1% | ≤0.1% | ≤0.2% | ≤1.0% |
| 50 | Fmoc-D-Tyr(Me)-OH | 201335-88-8 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 51 | I-Fmoc-N-Me-D-Tyr(tBu)-OH | 196808-79-4 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 52 | I-Fmoc-D-Tyr (Bzl)-OH | 138775-48-1 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 53 | I-Fmoc-D-Val-OH | 84624-17-9 | ≥98.5% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 54 | I-Fmoc-D-Hyp(tBu)-OH | 464193-92-8 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 55 | Fmoc-D-Thi-OH | 201532-42-5 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 56 | I-Fmoc-D-Tic-OH | 130309-33-0 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 57 | I-Fmoc-D-Oic-OH | 130309-37-4 | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 58 | Boc-D-His(Trt)-Aib-OH | NA | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 59 | I-Fmoc-D-Glu(OtBu)-Gly-OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 60 | U-Boc-D-His(Trt)-Aib-Glu(OtBu)-Gly-OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 61 | I-Boc-His(Trt)-Aib-D-Glu(OtBu)-Gly-OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 62 | U-Boc-D-His(Trt)-Aib-D-Glu(OtBu)-Gly-OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 63 | I-Fmoc-D-Arg(pbf)-Gly-OH | NA | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 64 | Fmoc-D-Ala-Ala-OH | NA | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 65 | Fmoc-Ala-D-Ala-OH | NA | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 66 | Fmoc-D-Ala-D-Ala-OH | NA | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 67 | I-Fmoc-D-Ls(Palm-Glu-OtBu)-OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 68 | I-Fmoc-Ls(Palm-D-Glu-OtBu)-OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 69 | I-Fmoc-D-Ls(Palm-D-Glu-OtBu)-OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 70 | I-Octa(OtBu)-D-Glu-OtBu | NA | ≥98.0% | ≤0.2% | ≤0.3% | ≤0.5% | ≤1.0% |
| 71 | I-Octa(OtBu)-D-Glu(ɑ-OtBu)-AEEA-AEEA-OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
*I-Max1 = Ubumsulwa obukhulu obungaziwa
Olunye Ulwazi:
I-Acetic Acid: ≤0.02% (Yonke Imikhiqizo)
I-Ethyl Acetate: ≤0.5% (Yonke Imikhiqizo)
- Utshwala: ≤0.5% (Yonke Imikhiqizo)
Amanzi Ahlanzekile
Amanzi ahlanzekile asetshenziswa ekukhiqizeni nasekuhlanzeni imishini ye-API.Amanzi ahlanziwe akhiqizwa ngamanzi edolobha, acutshungulwa ngokwelashwa kwangaphambili (isihlungi semidiya eminingi, isithambile, isihlungi se-carbon esicushiwe, njll.) kanye ne-osmosis ehlehlayo (RO), bese amanzi ahlanzekile agcinwa ethangini.Amanzi ahlala ezungeza ku-25±2℃ ngesilinganiso sokugeleza esingu-1.2m/s.
